Analytical Methodology
Mostrando 1-12 de 462 artigos, teses e dissertações.
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1. Study of Catalytic Pyrolysis of Biomass Sorghum (Sorghum bicolor L. Moench) Using Design of Experiments and Surface Response Methodology
This study proposes a screen of variables that have an influence on the modification of the bio-oil chemical composition as a unique critical quality attribute (CQA) throughout the pyrolytic process (zeolite, ZSM-5) by using a 24 full factorial design, followed by optimization through a response surface methodology (RSM) based on central composite design (CC
Journal of the Brazilian Chemical Society. Publicado em: 2023
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2. Eco-friendly multivariant green analytical technique for the estimation of ketoconazole by UV spectroscopy in bulk and cream formulation
The pharmaceutical industries are focusing on Green Analytical Chemistry principles like miniaturization, eco-friendly solvent usage, waste recycling, and analyst safety for sustainable results. A simple, eco-friendly sensitive and effective extraction and multivariant green analytical method to estimate ketoconazole in bulk and cream formulation were develo
Química Nova. Publicado em: 2022
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3. A Green Analytical Method Using Polyurethane Foam for The Extraction and Determination of Lauryl Ether Sulfate in Personal Care Hygiene Products
A green methodology was developed for the extraction and determination of lauryl ether sulfate in raw materials and commercial liquid soap and shower gel samples. The method avoids the use of organic solvents, offering a simple, cheap, and safe analysis. The methodology is based on the sorption of an ionic pair consisting of a cationic dye and an anionic sur
Journal of the Brazilian Chemical Society. Publicado em: 2022
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4. Analysis of Al2O3-ZrO2 ceramic insert in turning process of Ti-6Al-4V alloy using grey Taguchi-based response surface methodology (GT-RSM)
Abstract The present investigation aimed at a sustainable green turning operation of Ti-6Al-4V alloy using multi-objective optimization of surface roughness, tool flank wear, material removal rate, and tool wear loss with cutting speed, feed rate, and depth of cut as input parameters. The experiments were performed on a CNC lathe machine using an alumina-zir
Cerâmica. Publicado em: 2022
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5. Validation and Application of a Methodology for Quantifying Levels of Parabens in Sports Supplements from Brazil Using Liquid Chromatography-Mass Spectrometry
Although parabens have been reported to be used as antimicrobial preservatives in personal care products, pharmaceuticals, and foodstuffs, little is known about the occurrence of these compounds in sports supplements. In this study, a simple, fast and sensitive liquid chromatography tandem mass spectrometry method for simultaneous determination of five commo
Journal of the Brazilian Chemical Society. Publicado em: 2022
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6. A 2.4 GHz Coplanar Solar Cell Patch Antenna with a Semi-Analytical Evaluation of Temperature Effects
Abstract Solar cells integrated with antennas have aroused scientific interest as an attractive energy source alternative in low power devices for IoT and Wireless Sensor Network applications. Since the space for all components in the systems is scarce, different integration ideas have been proposed in this field. However, further analysis of the performance
Journal of Microwaves, Optoelectronics and Electromagnetic Applications. Publicado em: 2022
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7. Antecedent factors of violation of information security rules
Abstract Purpose This paper aims to investigate the influence of moral disengagement, perceived penalty, negative experiences and turnover intention on the intention to violate the established security rules. Design/methodology/approach The method used involves two stages of analysis, using techniques of structural equation modeling and artificial intellig
RAUSP Management Journal. Publicado em: 2022
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8. Electrochemical Determination of Trifluralin Herbicide Using Silver Solid Amalgam Electrode: Application in Fresh Food Samples
This paper reports the use of polished silver solid amalgam electrode (p-AgSAE) allied to square wave voltammetry (SWV) in the development of a simple, sensitive, fast and green electroanalytical methodology for the trifluralin herbicide determination in fresh food samples. The experimental (supporting electrolyte and potential and time accumulation) and vol
J. Braz. Chem. Soc.. Publicado em: 2021-07
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9. On the Use of a TiO2 Sol-Gel for Horseradish Peroxidase Enzyme Immobilization for Development of an Amperometric Biosensor
The sol-gel technique has drawn considerable attention in the area of biomolecules immobilization by virtue of its intrinsic properties including chemical inertness, thermal stability, and good biocompatibility. The present work reports the development of a bio-sensing methodology which involves the immobilization of horseradish peroxidase enzyme (HRP) on pe
J. Braz. Chem. Soc.. Publicado em: 2021-06
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10. COVID-19 and bleeding at unusual locations: Report of four cases
ABSTRACT Objectives The purpose of this study was to compare data obtained from the reticulocyte channel (RET channel) heated to 41 °C with those obtained from impedance channel (I-Channel) at room temperature in the samples with the mean corpuscular hemoglobin concentration (MCHC) < 370 g/L and in samples with the MCHC > 370 g/L, in the presence of cold a
Hematol., Transfus. Cell Ther.. Publicado em: 2021-06
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11. Use of the reticulocyte channel warmed to 41 °C of the XN-9000 analyzer in samples with the presence of cold agglutinins
ABSTRACT Objectives The purpose of this study was to compare data obtained from the reticulocyte channel (RET channel) heated to 41 °C with those obtained from impedance channel (I-Channel) at room temperature in the samples with the mean corpuscular hemoglobin concentration (MCHC) < 370 g/L and in samples with the MCHC > 370 g/L, in the presence of cold a
Hematol., Transfus. Cell Ther.. Publicado em: 2021-06
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12. UMA PROPOSTA PARA O ENSINO DE LABORATÓRIO DE QUÍMICA ANALÍTICA QUALITATIVA
Teaching laboratory of qualitative analytical chemistry is still a controversial issue in chemistry courses. However, important researchers and educators in chemistry recognized and highlighted the importance that the contents of this discipline represent in the formation of chemists, once it can provide handling and understanding of microscopic phenomena ba
Quím. Nova. Publicado em: 2021-04