Analytical Microscopy
Mostrando 1-12 de 115 artigos, teses e dissertações.
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1. A química analítica aplicada aos estudos de pigmentos rupestres: uma revisão
Instrumental advances have been employed in the study of archeological remains such as prehistoric rupestrians paintings with the objective of chemically characterizing them in order to reconstruct the cultural technologies of a prehistoric human group and/or to support conservation science studies. The analytical techniques most commonly used in archaeometr
Química Nova. Publicado em: 2022
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2. Microbial activity and studies on excavated megalithic micaceous potsherds from Peninsular India
Abstract The abundantly available mica flakes were added in raw materials to manufacture pottery in Central Peninsular India during the early Iron Age (700-300 BCE) for storage and glittering. The micaceous potsherds from the excavated megalithic site of Nagpur were studied for their composition, manufacturing techniques, microstructural features, microbial
Cerâmica. Publicado em: 2021-06
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3. A Simple Fluorescent Chemosensor for Detection of Zinc Ions in Some Real Samples and Intracellular Imaging in Living Cells
A new designed fluorescent chemosensor TYMN ((E)-1-((thiazol-2-ylimino)methyl)naphthalen-2-ol) for highly sensitive and selective tracing of trace amount of Zn2+ ions in some real samples was synthesized and characterized. The sensor TYMN can detect Zn2+ ions via fluorescence enhancement with a high selectivity over a wide range of metal ions, especially Cd2
J. Braz. Chem. Soc.. Publicado em: 2020-08
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4. Combined Analytical Py-GC/MS, SEM, FTIR and 13C NMR for Investigating the Removal of Trace Metals from Aqueous Solutions by Biochar
In this study, the efficiency of biochar (BC) produced from sugarcane bagasse at different pyrolysis temperatures (300, 400, 500 and 600 ºC) for simultaneous removal of CdII, PbII, CuII, CrIII, NiII and ZnII ions from aqueous solutions was assessed. All BC were characterized using scanning electron microscopy (SEM), Fourier transform infrared (FTIR), 13C nu
J. Braz. Chem. Soc.. Publicado em: 2020-07
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5. Chemically-Activated Biochar from Ricinus communis L. Cake and Their Potential Applications for the Voltammetric Assessment of Some Relevant Environmental Pollutants
Biochar is a rich-carbon material highly functionalized, which allows the use as electrodes modifier for preconcentration and voltammetric determination of several species. This work describes a castor cake biochar production and chemical activation with different reaction conditions using HNO3 and/or H2O2. Biochar samples were characterized using scanning e
J. Braz. Chem. Soc.. Publicado em: 2020-05
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6. Chemically Reduced Graphene Oxide on Gold Electrodes from Recordable CDs: Characterization and Potential Sensing Applications
This work presents the development and characterization of a new chemically modified electrode exploiting recordable Au-rewritable compact discs (AuCDs) as substrate for drop casting of a chemically-reduced graphene-oxide slurry focusing on simple and low-cost electrochemical sensors. Increase in electrochemical responses in cyclic voltammetric and amperomet
J. Braz. Chem. Soc.. Publicado em: 2020-03
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7. Synthesis of a Ce-Based MOF-76 with High Yield: A Study of Reaction Parameters Based on a Factorial Design
The purpose of this work was to optimize the synthesis yield of {[Ce(BTC)(H2O)]·DMF}n, a metal-organic framework (MOF)-76 family member, by solvothermal method. CeCl3.7H2O and 1,3,5-benzenetricarboxylic acid, 2:1 molar proportion, were added to N, N-dimethylformamide (DMF). Reaction time and temperature were evaluated to optimize the synthesis through a fac
J. Braz. Chem. Soc.. Publicado em: 2020-03
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8. Evaluation of a Graphite-Polyurethane Composite Electrode Modified with Copper Nanoparticles as an Amperometric Flow Detector in a Wall-Jet System for the Determination of Cysteine
A graphite-polyurethane composite electrode (GPUE) was modified by electrodeposition of copper nanoparticles (CuNP) followed by electrochemical treatment in NaOH (GPUE-CuNP), in order to prepare an amperometric sensor for the determination of cysteine (Cys). Cyclic votammograms of Cys solutions at GPUE-CuNP allowed the description of a sequence of electroche
J. Braz. Chem. Soc.. Publicado em: 2020-02
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9. Aço carbono 1040 como indicador de agressividade do solo e da pasta de cimento em sistemas de ancoragem de linhas de transmissão
RESUMO O encapsulamento de hastes de âncora em pasta de cimento reduz o contato dos materiais metálicos com os ambientes agressivos, em torres estaiadas de linhas de transmissão de energia elétrica. Contudo, ainda são reportados casos de falha prematura devido à corrosão do sistema de ancoragem. O íon cloreto é considerado um dos principais respons�
Matéria (Rio J.). Publicado em: 16/09/2019
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10. Synthesis of Hydrotalcite-Supported CdTe Semiconductor Nanocrystals for Electrochemical Detection of Ciprofloxacin
In this work, CdTe quantum dots (QDs) were controllably grown onto the surface of layered double hydroxide (LDH) aiming to develop a sensitive and selective method for the electrochemical detection of ciprofloxacin (CPX). Emission and absorption spectroscopy results as well as high-resolution transmission electron microscopy (HRTEM) images evidenced the form
J. Braz. Chem. Soc.. Publicado em: 23/05/2019
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11. Color electron microprobe cathodoluminescence of Bishunpur meteorite compared with the traditional optical microscopy method
Abstract Cathodoluminescence (CL) imaging is an outstanding method for sub classification of Unequilibrated Ordinary Chondrites (UOC) - petrological type 3. CL can be obtained by several electron beam apparatuses. The traditional method uses an electron gun coupled to an optical microscope (OM). Although many scanning electron microscopes (SEM) and electron
REM, Int. Eng. J.. Publicado em: 2018-04
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12. FOURIER TRANSFORM INFRARED SPECTROSCOPY, THERMOGRAVIMETRIC ANALYSIS, SCANNING ELECTRON MICROSCOPY AS SUPPORTING TOOLS IN QUALITY CONTROL OF ANTIPARASITICS
This study shows that Fourier transform infrared (FTIR) spectroscopy, thermogravimetric analysis (TGA), and scanning electron microscopy (SEM) can be used as supporting tools for the evaluation of the quality of antiparasitics. In addition, an analytical methodology was developed and validated to quantify simultaneously thiabendazole (TB), febantel (FB), tol
Quím. Nova. Publicado em: 2018-03