Chromatography On Paper
Mostrando 1-12 de 238 artigos, teses e dissertações.
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1. METHODS FOR EXTRACTION AND ISOLATION OF AGATHISFLAVONE FROM POINCIANELLA PYRAMIDALIS
Agathisflavone is a natural biflavone with restricted occurrence in plants. This biflavone presents several biological activities and can be important to developing new drugs. Obtaining such a molecule on a large scale for in vivo tests is a challenge. To date, there are no reports regarding its synthesis; thus, it is important to improve and develop methods
Química Nova. Publicado em: 2022
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2. The influence of cultivar and enzyme treatment on the aroma complex of apple juice
Abstract This paper aims to determine the influence of a cultivar (Golden delicious and Granny Smith) and enzyme treatments (hot and cold) on the aroma complex of clear apple juice. While the composition of aromatic components of the juice was determined by Gas Chromatography Mass Spectrometry (GC/MS) technique, a panel of 24 semi trained evaluators carried
Food Sci. Technol. Publicado em: 2021-06
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3. Avaliação da concentração e composição inorgânica do material particulado coletado no estado do Rio de Janeiro
Cities urbanization and modernization increase emission sources, contributing to particulate matter (PM) composition heterogeneity and enhance the risk to human health and environment. This paper intends to survey the studies on particulate matter carried out in the state of Rio de Janeiro. The sampling of PM is generally made using Hi-Vol samplers to collec
Quím. Nova. Publicado em: 2021-06
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4. Identification of Synthetic Drugs on Seized Blotter Papers Using ATR-FTIR and PLS-DA: Routine Application in a Forensic Laboratory
Blotter papers seizures containing synthetic drugs have intensified over the last decades. These drugs were originally conceived as “legal” alternatives to traditional illicit drugs, designed to mimic their effects and circumvent control agencies. Reference methods for determining these substances on blotter papers are based on chromatographic techniques
J. Braz. Chem. Soc.. Publicado em: 2021-03
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5. DETERMINATION OF CHEMICAL PROFILE OF Eugenia dysenterica ICE CREAM USING PS-MS AND HS-SPME/GC-MS
The incorporation of Cerrado fruits in food products such as ice cream has many advantages because it represents a source of nutrients and bioactive compounds. Given the demand for less laborious methods to analyze food, the paper spray ionization mass spectrometry technique was applied for the first time for a rapid characterization of the chemical componen
Quím. Nova. Publicado em: 2021-02
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6. Synthesis of Hybrid Monolithic Columns Using a Click Chemistry Reaction for Application in Capillary Liquid Chromatography
Hybrid monolithic columns present characteristics of both silica and organic monoliths, such as good mechanical properties, wide pH tolerance, high permeability and stability and little swelling or shrinkage. A common way to prepare this type of material is by using alkoxysilanes and organic monomers via the sol-gel process and click chemistry reactions. In
J. Braz. Chem. Soc.. Publicado em: 24/10/2019
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7. TARGETED AND NON-TARGETED ANALYSIS BASED ON ULTRA HIGH PERFORMANCE LIQUID CHROMATOGRAPHY AND FOURIER TRANSFORM INFRARED SPECTROSCOPY FOR PARIS SPECIES OF DIFFERENT GEOGRAPHICAL ORIGINS
Various species of Paris have been used in treatments for their antitumor, antimicrobial, hemostatic, anthelmintic and immune-stimulating properties, among others. The bioactive markers of these plants including paris saponins I (PSI), paris saponins II (PSII), paris saponins VI (PSVI) and paris saponins VII (PSVII) are responsible for inhibiting nasopharyng
Quím. Nova. Publicado em: 27/05/2019
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8. Assessment of Novel C-4 Methylated Tetraketide by HPLC-SPE-TT in Saccharicola sp., an Endophytic Fungus in Eugenia jambolana Lam.
A new compound named methyl (6S,7S,2E,4E)-6,7-dihydroxy-4,6-dimethyl octanoate was isolated from Saccharicola sp. using high performance liquid chromatography-solid phase extraction-transfer tube (HPLC-SPE-TT), together with four known compounds, fusaric acid, trans-4-hydroxymellein, thymidine and adenosine. Saccharicola sp. was isolated from the stems of Eu
J. Braz. Chem. Soc.. Publicado em: 2019-03
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9. Catalytic Cracking of Soybean Oil for Biofuel over γ-Al2O3/CaO Composite Catalyst
In this paper, we report the catalytic cracking of soybean oil for biofuel over γ-Al2O3/CaO composite catalysts. The influence of catalysts, cracking temperature and weight hourly space velocity (WHSV) on the products distribution were investigated. The maximum yield (70.0 wt.%) of biofuel with low acid value (6.7 mg KOH g-1) and oxygen content (5.6%), as w
J. Braz. Chem. Soc.. Publicado em: 2019-02
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10. Screening and Binding Analysis of Flavonoids with Alpha-Amylase Inhibitory Activity from Lotus Leaf
Lotus leaf is gaining growing popularity due to its various benefits and widely usage. In this paper, ten flavonoids in lotus leaf extract were analyzed by high performance liquid chromatography (HPLC). Centrifugal ultrafiltration combined liquid chromatography was used to screen alpha-amylase inhibitors from ten flavonoids mixture and the binding degrees ra
J. Braz. Chem. Soc.. Publicado em: 2018-03
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11. GC-FID METHODOLOGY VALIDATION FOR THE FATTY ESTERS CONTENT DETERMINATION IN BIODIESEL WITH HEXADECYL ACETATE AS THE INTERNAL STANDARD
Biodiesel purity expressed as fatty esters content is one of its most important quality parameters. Although several instrumental methods have been employed, gas chromatography with internal standard calibration has been the most used. Biodiesel is a very complex matrix, therefore finding a suitable internal standard (IS) is not straightforward. EN14103:2003
Quím. Nova. Publicado em: 2017-09
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12. Preparative Separation and Structural Identification of Impurities of a New α2-Adrenoceptor Agonist Using Stacking Injection, LC-MSn and LC-SPE-NMR
Identifying impurities in drug substances has become one of the most important issues in pharmaceutical analysis since it can have a significant impact on the efficacy of new pharmaceutical products. Due to the purity requirements, in this paper a new synthetic α2-adrenoceptor agonist, called LPSF-PT-31, was purified and its impurities were characterized by
J. Braz. Chem. Soc.. Publicado em: 2017-06