Epma
Mostrando 1-12 de 19 artigos, teses e dissertações.
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1. Nb-Al Binary System: Reevaluation of the Solubility Limits of the (Nb), Nb3Al, Nb2Al and NbAl3 Phases at High Temperatures
In this work a re-investigation of the solubility limits of the (Nb), Nb3Al, Nb2Al and the Nb-rich side of the NbAl3 phases on the Nb-Al system is presented. Alloys in the binary fields ((Nb)+Nb3Al, Nb3Al+Nb2Al and Nb2Al+NbAl3) were arc-melted, and then equilibrated at 1000, 1200 and 1400 ºC. The phases were confirmed via X-ray powder diffractometry, and th
Mat. Res.. Publicado em: 25/11/2019
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2. Microstructure and Wear Resistance of ZrC-ZrB2 /Ni Composite Coatings Prepared by Plasma Transferred Arc Cladding
The ZrC-ZrB2/Ni metal matrix composite coatings were in-situ synthesized from a mixture of Ni, Zr and B4C by plasma transferred arc (PTA) cladding process. Microstructures and phase constituents of the coatings were characterized by electron probe micro-analyzer (EPMA) and X-ray diffraction (XRD). Microhardness and wear resistance of the coatings were system
Mat. Res.. Publicado em: 06/05/2019
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3. Influence of Forging Pressure on Microstructural and Mechanical Properties Development in Linear Friction Welded Al-Cu Dissimilar Joint
Abstract Dissimilar AA5083 and C101 pure copper linear friction welds were prepared using different forging pressures (60 MPa, 80 MPa, and 110 MPa) to investigate the influence of the forging pressure on the microstructural and mechanical properties development using optical microscopy (OM), scanning electron microscopy (SEM), hardness measurements, and ten
Soldag. insp.. Publicado em: 18/04/2019
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4. Color electron microprobe cathodoluminescence of Bishunpur meteorite compared with the traditional optical microscopy method
Abstract Cathodoluminescence (CL) imaging is an outstanding method for sub classification of Unequilibrated Ordinary Chondrites (UOC) - petrological type 3. CL can be obtained by several electron beam apparatuses. The traditional method uses an electron gun coupled to an optical microscope (OM). Although many scanning electron microscopes (SEM) and electron
REM, Int. Eng. J.. Publicado em: 2018-04
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5. Identification of Heavy Metals in Crystals of Sand and Silt Fractions of Soils by Scanning Electron Microscopy (SEM EDS/WD-EPMA)
ABSTRACT Studies of heavy metals are concentrate on clay fractions, but coarser fractions of the soil can constitute significant sources of structural forms of heavy metals. The aim of this study was to evaluate the occurrence of heavy metals in the structure of minerals of the sand and silt fractions of soils from three different parent materials (metamorph
Rev. Bras. Ciênc. Solo. Publicado em: 08/03/2018
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6. Effect of Ferrite on the Precipitation of σ Phase in Cast Austenitic Stainless Steel Used for Primary Coolant Pipes of Nuclear Power Plants
The effect of ferrite phase on the precipitation of σ phase in a Z3CN20.09M cast austenitic stainless steel (CASS) used for primary coolant pipes of pressurized water reactor (PWR) nuclear power plants was investigated by using isothermal heat-treatment, optical microscopy (OM), transmission electron microscopy (TEM) and electron probe microanalysis (EPMA)
Mat. Res.. Publicado em: 28/09/2017
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7. Study on the NaOH/metakaolin Ratio and Crystallization Time for Zeolite a Synthesis from Kaolin Using Statistical Design
The NaOH/metakaolin ratio and crystallization time were studied for the synthesis of zeolite NaA from a sample of kaolin from a Capim mine. The tests were carried out by using statistical design with axial points and replication of the central point. The samples obtained were characterized by X-ray diffraction (DRX), scanning electron microscopy and chemical
Mat. Res.. Publicado em: 13/04/2017
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8. Retrieval analysis of different orthodontic brackets: the applicability of electron microprobe techniques for determining material heterogeneities and corrosive potential
OBJECTIVE: The objective of this study was to investigate the applicability of micro-analytical methods with high spatial resolution to the characterization of the composition and corrosion behavior of two bracket systems. MATERIAL AND METHODS: The surfaces of six nickel-free brackets and six nickel-containing brackets were examined for signs of corrosion an
J. Appl. Oral Sci.. Publicado em: 2012-08
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9. Geoquímica de Sills Basálticos da formação Serra Geral, sul do Brasil, com base em rocha total e micro-análise de minerais
O grande magmatismo intracontinental ocorrido a 133 Ma na Bacia do Paraná foi desenvolvido por um sistema fissural no qual a interação da Pluma Tristão da Cunha na base da litosfera (com ou sem contaminação crustal) gerou derrames, diques e sills no Brasil, nos Estados do RS, SC, PR, SP, MT, MS e GO, e em parte do Paraguai, Argentina e Uruguai. Na Form
Publicado em: 2010
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10. Metalocenos suportados para a polimerização de etileno: efeito do uso de espaçadores na superfície da sílica
A homopolimerização de etileno foi investigada utilizando o catalisador (nBuCp)2ZrCl2 suportado em sílicas modificadas quimicamente com diferentes espaçadores. Dentre eles, foram utilizados Me3SiCl, Me2HSiCl, Ph3SiCl, polimetilhidrossiloxano (PMHS), GeCl4, SnCl4 ou PbCl2. As interações organossilano-sílica, zirconoceno-silanos suportados e zirconoceno
Publicado em: 2009
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11. NewIn-situ synthesis method of magnesium matrix composites reinforced with TiC particulates
Magnesium matrix composites reinforced with TiC particulates was prepared using a new in-situ synthesis method of remelting and dilution technique. And measurements were performed on the composites. The results of x ray diffraction (XRD) analysis confirmed that TiC particulates were synthesized during the sintering process, and they retained in magnesium mat
Materials Research. Publicado em: 2006-12
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12. Efeito magnetocalorico em filmes finos nanocompositos sintetizados por sputtering / Magnetocaloric effect in nanocomposite thin films obtained by sputtering
The magnetic properties of films obtained by the co-deposition of a ferromagnetic and a non-magnetic components are the subject of intense investigation. In this work, the magnetic properties of Gdx W1-x, with x ranging from 0 to 1, were investigated. The films were deposited by magnetron sputtering from Gd and W targets. EPMA (electron probe microanalysis)
Publicado em: 2006