Experimental Design Composite
Mostrando 1-12 de 129 artigos, teses e dissertações.
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1. PLANEJAMENTO FATORIAL NA SÍNTESE DO OLEATO DE ETILA CATALISADA PELA LIPASE NATIVA DE Aspergillus niger
This work reports the use of the Octave, a free computational software, to optimize the experimental design in the synthesis of ethyl oleate from oleic acid and ethanol catalyzed by a native lipase from Aspergillus niger. The central composite factorial design (CCD) was performed with 2 levels and 3 variables (temperature, mass of native A. niger lipase and
Química Nova. Publicado em: 2022
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2. OPTIMIZATION OF BREWING WASTE’S (TRUB) PHENOLIC COMPOUNDS EXTRACTION BY ULTRASOUND ASSISTED USING RESPONSE SURFACE METHODOLOGY
The brewing waste, also known as trub, is an abundant by-product of the brewing industry. Such material presents high levels of phenolic compounds, which promote antioxidant, antimicrobial and antifungal effects, turning the trub economically attractive. In this study, the trub’s phenolic compounds were extracted by ultrasound-assisted extraction technolog
Quím. Nova. Publicado em: 2021-04
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3. Impact responses of slender composite plates for bird-strike testing of fan blades
Abstract Bird-strike failure of fan blades is one of the basic challenges for the safety of aircraft engines. Simplified slender blade-like plates are always used to evaluate the impact-induced damage mechanism at design stage. One undesirable issue is the failure at the root of clamped slender plates, which cannot recover the real case of twisted blades. Fo
Lat. Am. j. solids struct.. Publicado em: 04/11/2019
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4. Application of quality by design approach in RP-HPLC method development for simultaneous estimation of saxagliptin and dapagliflozin in tablet dosage form
A simple, sensitive, precise, accurate and robust high performance liquid chromatographic method has been developed for simultaneous estimation of saxagliptin (SAXA) and dapagliflozin (DAPA) in pharmaceutical formulation. Design of experiments (DoE) was applied for multivariate optimization of the experimental conditions of RP-HPLC method. Risk assessment wa
Braz. J. Pharm. Sci.. Publicado em: 24/10/2019
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5. Optimal condition of cannabis maceration to obtain the high cannabidiol and Δ9-tetrahydrocannabinol content
Abstract: The aim of this work was to optimize a maceration condition of cannabis (Cannabis sativa L.). A circumscribed central composite experimental design was applied in this work. Temperature and time were varied from 40-80 °C and 30-90 min, respectively. The three responses (i.e., extraction yield, cannabidiol content, and Δ9- tetrahydrocannabinol con
An. Acad. Bras. Ciênc.. Publicado em: 14/10/2019
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6. APPLICATION OF RESPONSE SURFACE METHODOLOGY FOR LIPASE CATALYZED SYNTHESIS OF 2-ETHYLHEXYL PALMITATE IN A SOLVENT FREE SYSTEM USING ULTRASOUND
Abstract This study aims at clean production of 2-ethylhexyl palmitate catalyzed by lipase Fermase CALB 10000 in a solvent-free system using ultrasound technology. The central composite design (CCD) of response surface methodology with 4 factors at 3 levels consisting of acid to alcohol molar ratio (1:3-1:7), enzyme loading (3 %-7% (w/w)), ultrasound power (
Braz. J. Chem. Eng.. Publicado em: 30/09/2019
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7. Preparação, caracterização e avaliação catalítica do compósito Fe2O3/grafite em reação foto-Fenton
RESUMO Neste trabalho, compósito Fe2O3/grafite foi preparado e usado como um catalisador em reação foto-Fenton para a descoloração de solução aquosa contendo o corante amaranto sob irradiação de luz visível. Amostras com diferentes teores de Fe2O3 suportados sobre grafite foram preparadas e caracterizadas por difração de raios-X (DRX), adsorção
Matéria (Rio J.). Publicado em: 16/09/2019
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8. Uso da metodologia de superfície de resposta na otimização da extração de compostos fenólicos da casca dos frutos de Hymenaea courbaril L. (Jatobá)
Resumo Os hábitos alimentares e medicinais dos povos da região Amazônica são ricos em frutos considerados exóticos ou subutilizados comercialmente, alguns dos quais geram considerável quantidade de resíduos. As cascas do fruto de Hymenaea courbaril L. (jatobá) foram submetidas a um processo de extração simultânea de compostos fenólicos, otimizado
Braz. J. Food Technol.. Publicado em: 12/09/2019
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9. Effects of Resistance Exercise with Instability on Neurocognitive Functions (REI STUDY): Study Protocol for a Proof-of-Concept Clinical Trial in Older Adults with Subjective Cognitive Complaints
Abstract Aim: Resistance exercise (RE) is a widely accepted strategy to counteract the effects of aging and chronic diseases on health-related outcomes. Studies have been suggested that RE improves brain and cognitive health. RE with unstable devices (REI) is a neuromotor complexity strategy with the potential to improve strength, power, and balance in onde
Motriz: rev. educ. fis.. Publicado em: 26/08/2019
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10. Comparison of acid and enzymatic hydrolysis of pectin, as inexpensive source to cell growth of Cupriavidus necator
Abstract: The present work investigated what the appropriate methods of hydrolysis of pectin for reducing compounds (RCs) production, employed as a substrate for cell growth of Cupriavidus necator. This microorganism has great importance industrial, because besides potential single cell protein (SCP), is the most studied microorganism for production of polyh
An. Acad. Bras. Ciênc.. Publicado em: 25/04/2019
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11. Investigation on influence of stamp forming parameters on formability of thermoplastic composite
Abstract Advanced fabric reinforced polymer composites find extensive applications in aerospace and structural fields due to their high mechanical properties. A novel stamp forming technique finds extensive use in the hemispherical forming of thermoplastic composites. This study investigates the influence of stamp forming parameters on the formability of th
Polímeros. Publicado em: 29/11/2018
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12. Use of Experimental Design to Evaluate the Effect of the Incorporation of Quartzite Residues in Ceramic Mass for Porcelain Tile Production
The potential of using quartzite residues in the composition of an industrial ceramic mass for porcelain tile production was investigated through experimental design. Chemical, physical and microstructural analyses were accomplished to understand how the incorporation of quartzite residues affects the material, before and after sintering. Central composite d
Mat. Res.. Publicado em: 29/10/2018