Extraction Columns
Mostrando 1-12 de 102 artigos, teses e dissertações.
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1. A Systematic Pipeline to Enhance the Fecal Metabolome Coverage by LC-HRMS
The comprehended knowledge of the metabolic profile of the fecal matter has been recognized as an important point for understanding metabolic changes in the human systemic metabolism and it can provide precious information about host-gut microbiota interactions. However, few analytical strategies have been addressed for a broad analysis of metabolites with d
J. Braz. Chem. Soc.. Publicado em: 2021-07
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2. An Online Solid Phase Extraction-Liquid Chromatography Tandem Mass Spectrometry Method for the Analysis of Parabens in Urban Waters
In this work, we report a method to quantify methylparaben, ethylparaben, propylparaben and butylparaben in urban waters of São Carlos (São Paulo State, Brazil) by online solid phase extraction-liquid chromatography tandem mass spectrometry (SPE-LC-MS/MS) system. The method achieved ng L-1 limits with good accuracy and precision (internal standards for eac
J. Braz. Chem. Soc.. Publicado em: 2021-05
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3. Potential Slow Release Fertilizers Based on K2MgSiO4 Obtained from Serpentinite
In this work, a potassium magnesium silicate mineral based on phase K2MgSiO4 was prepared from serpentinite rock and studied as a potential K and Mg slow-release fertilizer. The material was prepared by impregnation of serpentinite/KOH and calcination at 700 °C to produce K2MgSiO4 phase, olivine and forsterite. The release patterns of K and Mg in the stirre
J. Braz. Chem. Soc.. Publicado em: 2020-04
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4. Development and characterization of an immunoaffinity column for the detection of danofloxacin residues in milk samples
Abstract In this study, an immunoaffinity column was prepared by covalently coupling of polyclonal antibody against danofloxacin (DAN) with chitosan microparticles and its potential application to selective extraction of DAN from food samples was also evaluated. The produced antibody exhibited high sensitivity, with an IC50 value of 4.56 ng/mL towards DAN,
Food Sci. Technol. Publicado em: 30/07/2018
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5. Solid-phase extractions in flow analysis
ABSTRACT Coupling solid-phase extraction (SPE) to flow systems has promoted a synergistic development. Whereas SPE mechanization leads to improved precision and higher sample throughput, as well as diminishes systematic errors and contamination risks, analyte concentration and separation from the sample matrix provides a remarkable impact on detectability an
An. Acad. Bras. Ciênc.. Publicado em: 2018
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6. PERFORMANCE OF TIFTON 85 GRASS UNDER FERTIRRIGATION WITH SLAUGHTERHOUSE WASTEWATER
ABSTRACT: The aim of this study was to evaluate the performance of Tifton 85 grass cultivated in soil columns and fertilized with different wastewater doses of swine slaughterhouse. The experiment was conducted in the Environmental Engineering Center and Sanitary of UFLA/MG in PVC columns filled with Dark Red Latosol (Oxisol) and randomly distributed. The tr
Eng. Agríc.. Publicado em: 2017-08
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7. A Simple and Fast Method for Magnetic Solid Phase Extraction of Ochratoxin A
We report on the synthesis of dopamine loaded magnetic nanoparticles (MNPs) for new, simple, fast and repeatable extraction of ochratoxin A from different solvents and milk without utilizing immunoaffinity columns and even high-tech devices. To this end, Fe3O4 nanoparticles (NPs) were synthesized using thermal decomposition reaction and dopamine (DPA) was th
J. Braz. Chem. Soc.. Publicado em: 2017-06
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8. HS-SPME optimization and extraction of volatile compounds from soursop (Annona muricata L.) pulp with emphasis on their characteristic impact compounds
Abstract Aroma and taste are decisive factors in the selection of any food. The aim of this study was to extract the volatile compounds present in soursop (Annona muricata L.) pulp by Solid-phase microextraction (SPME) technique using 3 different fibers (DVB/CAR/ PDMS, CAR/PDMS and PDMS/DVB). An experimental design was set up to evaluate the best extraction
Food Sci. Technol. Publicado em: 29/05/2017
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9. Application of HPLC-DAD for the quantification of Lycorine in Galanthus elwesii Hook
ABSTRACT In the present study, a reversed-phase high-performance liquid chromatographic method has been used for the quantitative determination of lycorine in the aerial parts and bulbs of G. elwesii Hook. A simple method for the extraction of lycorine in low mass plant samples was employed utilizing pre-packed columns with diatomaceous earth (Extrelut(r)).
Braz. J. Pharm. Sci.. Publicado em: 20/04/2017
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10. Quantificação de alquilbenzeno linear sulfonato em estação de tratamento de efluentes e rios por cromatografia líquida de alta eficiência e extração em fase sólida
The procedures to implement a chromatographic method for the quantification of linear alkyl benzene sulfonate (LAS) in the influent, effluent and sludge of a wastewater treatment plant (WWTP), and in river water and sediment, are described and evaluated. The columns octylsilane (C8) and octadecylsilane (C18) for high performance liquid chromatography were ev
Quím. Nova. Publicado em: 2017-04
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11. Boron Leaching Decreases withIncreases on Soil pH
ABSTRACT Management of boron fertilization depends on the magnitude of B leaching in the soil profile, which varies proportionally with the concentration of B in the soil solution, which, in turn, decreases as the soil pH increases due to the higher sorption of B on soil solid surfaces. The objective of this study was to quantify the effect of liming and rat
Rev. Bras. Ciênc. Solo. Publicado em: 26/04/2016
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12. Evaluation of Monolithic and Core-Shell Columns for Separation of Triazine Herbicides by Reversed Phase High Performance Liquid Chromatography
Monolithic and core-shell columns were comparatively evaluated for separation of deisopropylatrazine (DIA), deethylatrazine (DEA), hydroxyatrazine (HAT), simazine (SIM) and atrazine (ATR) under similar conditions of elution, flow rate and sample volume. Although both columns provided separation of the analytes with resolution > 1.5, the core-shell column exh
J. Braz. Chem. Soc.. Publicado em: 2015-11