Linearity Test
Mostrando 1-12 de 90 artigos, teses e dissertações.
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1. Validation of an UHPLC-MS/MS Method for the Determination of Malachite Green, Leucomalachite Green, Crystal Violet, and Leucocrystal Violet in Shrimp, Fish, and Salmon Muscle Using a Modified QuEChERS Approach
A quantitative and confirmatory method for detecting the presence of triphenylmethane dyes in shrimp muscle using ultra-high performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) and a quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction approach was validated. The method exhibited linearity and selectivity and the coeffici
J. Braz. Chem. Soc.. Publicado em: 2021-04
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2. TITULADOR AUTOMÁTICO EM FLUXO-BATELADA UTILIZANDO UM HARDWARE DE CÓDIGO FONTE ABERTO ARDUINO
This work describes the development of an automatic titrometric method in flow-batch with potentiometric detection using alternative and easily accessible materials. Arduino board and its modules, solenoid valves to control the flow rate, peristaltic pump to propel and suction fluids and tubes of inert material to connect the different parts of the Flow-Batc
Quím. Nova. Publicado em: 2021-03
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3. Quantification of Arsenic, Cadmium, Mercury and Lead in Pineapple: Method Development, Validation and Evaluation of In-House Reference Materials
A method for quantification of arsenic, cadmium, mercury, and lead in pineapple using inductively coupled plasma-mass spectrometry (ICP-MS) was developed, validated, and used to test the homogeneity and stability of in-house reference materials. The method was tested at the regulation levels given by the Food and Agriculture Organization of the United Nation
J. Braz. Chem. Soc.. Publicado em: 2020-06
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4. Simultaneous determination of anti-diabetic drugs
A novel reverse phase, isocratic HPLC method is described to separate five anti-diabetic drugs i.e., glimepiride, metformin, sitagliptin, rosiglitazone and pioglitazone. Nucleosil C18 analytical column was used as stationary phase, while mobile phase consisted of acetonitrile:phosphate buffer: methanol (40/40/20, v/v) pH 2.0. Effluent was monitored at a flow
Braz. J. Pharm. Sci.. Publicado em: 20/12/2019
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5. DETERMINATION OF INDIVIDUAL GLUCOSE THRESHOLD USING PHARMACY PORTABLE BLOOD GLUCOSE METER
RESUMO Introdução O limiar glicêmico individual (LGI) tem sido utilizado para estimar o limiar anaeróbico com baixo custo das análises e também em menor tempo. Entretanto, dá-se pouca atenção para a confiabilidade das análises glicêmicas por meio do glicosímetro portátil de farmácia. Objetivo Determinar o LGI por meio de glicosímetro port�
Rev Bras Med Esporte. Publicado em: 01/07/2019
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6. Analytical validation of real-time quantitative PCR assays for optimum diagnosis of vivax malaria
BACKGROUND The prompt diagnosis of plasmodial species for effective treatment prevents worsening of individual health and avoids transmission maintenance or even malaria reintroduction in areas where Plasmodium does not exist. Polymerase chain reaction (PCR) allows for the detection of parasites below the threshold of microscopic examination. OBJECTIVE O
Mem. Inst. Oswaldo Cruz. Publicado em: 31/01/2019
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7. Measurement uncertainty of plane-strain fracture toughness KIC testing by the Monte Carlo Method
Abstract The reliable determination of materials' mechanical properties is a fundamental factor for their application in engineering, and the estimation of the measurement uncertainty in testing laboratories has a direct impact on the interpretation of the results. Recent literature demonstrates that one of the most widely used methodologies for uncertainty
REM, Int. Eng. J.. Publicado em: 2018-04
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8. Spectrophotometric determination of rosuvastatin in pharmaceutical formulations using quinalizarin
ABSTRACT This work presents the development of a methodology based on the formation of a charge transfer complex between quinalizarin and rosuvastatin, allowing for the spectrophotometric determination of rosuvastatin at 579 nm. The factors involved in the sensitivity of the technique were studied (nature and proportion of the solvent, reaction time, pH of a
Braz. J. Pharm. Sci.. Publicado em: 31/07/2017
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9. Validation of spectrophotometric microplate methods for polyphenol oxidase and peroxidase activities analysis in fruits and vegetables
Abstract Enzymes polyphenol oxidase (PPO) and peroxidase (POD) play important roles in the processing of fruits and vegetables, since they can produce undesirable changes in color, texture and flavor. Classical methods of activity assessment are based on cuvette spectrophotometric readings. This work aims to propose, to validate and to test microplate spectr
Food Sci. Technol. Publicado em: 25/05/2017
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10. Soil Organic Carbon Determination Using NIRS: Evaluation of Dichromate Oxidation and Dry Combustion Analysis as Reference Methods in Multivariate Calibration
Dichromate oxidation and dry combustion analysis were evaluated as reference methods to determine organic carbon in Brazilian soils using near infrared spectroscopy (NIRS) as an alternative. The main objective of this study was to evaluate which of the reference methods could provide a calibration model with higher predictive ability. A total of 161 soil sam
J. Braz. Chem. Soc.. Publicado em: 2016-09
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11. Development, Optimization and Validation of an HPLC-PDA Method for Quantification of Taxifolin in the Bark Extract of Pinus pinaster
The aqueous extract of the bark of Pinus pinaster has a high concentration of polyphenols represented by a mixture of procyanidins, besides taxifolin, phenolic acids, cinnamic acids and their glycosides. Its quality control is specified in the United States Pharmacopeia, and the assay test is performed by determination of the total procyanidins content. Howe
J. Braz. Chem. Soc.. Publicado em: 2016-09
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12. On the Validation of a Numerical Model for the Analysis of Soil-Structure Interaction Problems
Abstract Modeling and simulation of mechanical response of structures, relies on the use of computational models. Therefore, verification and validation procedures are the primary means of assessing accuracy, confidence and credibility in modeling. This paper is concerned with the validation of a three dimensional numerical model based on the finite element
Lat. Am. j. solids struct.. Publicado em: 2016-08