Micro Raman Spectroscopy
Mostrando 1-12 de 55 artigos, teses e dissertações.
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1. NANOESPECTROSCOPIA DE ABSORÇÃO DE RADIAÇÃO SÍNCROTRON NO INFRAVERMELHO PARA NANOESPECIAÇÃO DE PRODUTOS DE CORROSÃO METÁLICA
The understanding of chemical and physical behavior of materials, especially metals and their alloys, is of utmost importance for industrial and technological applications, development of new materials and preservation of cultural heritage. The use of complementary analytical techniques has allowed a better understanding of corrosion mechanisms, and results
Quím. Nova. Publicado em: 05/12/2019
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2. Microwave radiation influence on the thermal and spectroscopic properties of Na-birnessite-type material
Resumo No presente trabalho, apresenta-se um estudo da influência da radiação micro-ondas nas propriedades térmica e espectroscópica, assim como estrutural (ordem-desordem) e morfológica, de óxido de Mn estruturado em camada tipo Na-birnessita. A rota empregada para obtenção da matriz lamelar foi a precipitação redox. Os produtos foram caracteriza
Cerâmica. Publicado em: 14/11/2019
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3. Apatite multi-generations in the Três Estradas Carbonatite, Southern Brazil: physical and chemistry meaning and implications to phosphate ore quality
Abstract Carbonatites were recently discovered in Southern Brazil, which increased the interest to evaluate the economic potential of these uncommon rocks, especially the Três Estradas Carbonatite. Carbonates are the dominant minerals of fresh rock followed by apatite, but the weathering process makes apatite abundant. We focused on apatite from the carbona
Braz. J. Geol.. Publicado em: 01/07/2019
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4. Effects of experimental bleaching agents on the mineral content of sound and demineralized enamels
Abstract High concentrations of hydrogen peroxide can cause adverse effects on composition and structure of teeth. However, the addition of calcium and fluoride in bleaching agents may reduce enamel demineralization. Objective: To evaluate chemical changes of sound and demineralized enamels submitted to high concentrations of hydrogen peroxide containing fl
J. Appl. Oral Sci.. Publicado em: 04/10/2018
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5. Annealing Effects on the Structural and Optical Properties of ZnO Nanostructures
ZnO nanostructures were synthesized by a proteic sol-gel method, using zinc nitrate hexahydrate and gelatin as precursors. Size and shape evolution of ZnO nanostructures were achieved by annealing temperature in the range 250-1000 ºC. The crystalline structure, morphology and optical properties of the ZnO nanoparticles were characterized by X-Ray Diffractio
Mat. Res.. Publicado em: 05/03/2018
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6. Mineral inclusions in diamonds from Chapada Diamantina, Bahia, Brazil: a Raman spectroscopic characterization
Abstract The Chapada Diamantina, located in the central region of the State of Bahia, is of important historical significance due to its diamond occurrences. Discovered in the nineteenth century, comprehensive research about the regional diamonds and their origins are still limited, demanding more investigation in the matter. Looking for insights about their
REM, Int. Eng. J.. Publicado em: 2018-03
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7. Effect on adhesion of a nanocapsules-loaded adhesive system
Abstract This study aimed to evaluate the in situ degree of conversion, contact angle, and immediate and long-term bond strengths of a commercial primer and an experimental adhesive containing indomethacin- and triclosan-loaded nanocapsules (NCs). The indomethacin- and triclosan-loaded NCs, which promote anti-inflammatory and antibacterial effects through co
Braz. oral res.. Publicado em: 01/02/2018
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8. Pre-sintered Y-TZP sandblasting: effect on surface roughness, phase transformation, and Y-TZP/veneer bond strength
Abstract Sandblasting is a common method to try to improve the Y-TZP/veneer bond strength of dental prostheses, however, it may put stress on zirconia surfaces and could accelerate the t→m phase transformation. Y-TZP sandblasting before sintering could be an alternative to improve surface roughness and bonding strength of veneering ceramic. Objectives. Th
J. Appl. Oral Sci.. Publicado em: 2017-12
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9. Influence of curing protocol and ceramic composition on the degree of conversion of resin cement
Abstract Due to increasing of aesthetic demand, ceramic crowns are widely used in different situations. However, to obtain long-term prognosis of restorations, a good conversion of resin cement is necessary. Objective: To evaluate the degree of conversion (DC) of one light-cure and two dual-cure resin cements under a simulated clinical cementation of cerami
J. Appl. Oral Sci.. Publicado em: 2017-12
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10. Effect of Heat Treatments and SiC Content in the Mechanical Properties and Microstructure of Self-Lubricating Steels
The objective of the present work was to study the effect of heat treatments in the microstructure, graphite nodules and mechanical properties of self-lubricating steels, to achieve this, self-lubricating steels (Fe + 0.45C + 4Ni + 1Mo %wt) and additions of 2 and 3 %wt SiC were fabricated. They were consequently heat treated in 3 different conditions: martem
Mat. Res.. Publicado em: 09/11/2017
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11. Physical Vapor Deposited Films of a Perylene Derivative: Supramolecular Arrangement and Thermal Stability
The analysis of supramolecular arrangement is essential to understand the role of this key factor on the optical and electrical properties of organic thin films. In this work, thin solid films of bis(phenethylimido) perylene (PhPTCD) fabricated using physical vapor deposition (PVD) technique (thermal evaporation), deposited simultaneously onto different subs
Mat. Res.. Publicado em: 23/03/2017
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12. Síntese de BaTIO3 e SrTIO3 pelo método hidrotermal assistido por micro-ondas utilizando anatase como precursor de titânio
In this work barium titanate (BT) and strontium titanate (ST) were prepared by Microwave-Assisted Hydrothermal (MAH) method, using a Ti precursor different from those shown in the literature and various concentrations (1, 3 e 6 mol L-1) of KOH mineralizer. As a titanium precursor, an anatase complex with hydrogen peroxide were used. For the precursors of bar
Quím. Nova. Publicado em: 2017-02