Monolithic Columns
Mostrando 1-11 de 11 artigos, teses e dissertações.
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1. Synthesis of Hybrid Monolithic Columns Using a Click Chemistry Reaction for Application in Capillary Liquid Chromatography
Hybrid monolithic columns present characteristics of both silica and organic monoliths, such as good mechanical properties, wide pH tolerance, high permeability and stability and little swelling or shrinkage. A common way to prepare this type of material is by using alkoxysilanes and organic monomers via the sol-gel process and click chemistry reactions. In
J. Braz. Chem. Soc.. Publicado em: 24/10/2019
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2. Damage index analysis of prefabricated segmental bridge columns under cyclic loading
Abstract The damage index is usually applied to evaluate the damage states of bridge structures, which is the basis of structural fragility study. The present study investigates the seismic damage index of the prefabricated segmental bridge columns (PSBC) under cyclic loading by theoretical and numerical analysis. Based on the previous pseudo-static experime
Lat. Am. j. solids struct.. Publicado em: 03/12/2018
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3. Coupled monolithic columns as an alternative for the use of viscous ethanol–water mobile phases on chromatographic fingerprinting complex samples
ABSTRACT Concepts of sustainability have received attention from people involved in investigation of nature-derived matrices. The effects of concomitant pollutant activities are cumulative and harmful to the environment from which these matrices are obtained. High performance liquid chromatography analyses generate millions of litters of chemical waste world
Rev. bras. farmacogn.. Publicado em: 2018-06
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4. Evaluation of Monolithic and Core-Shell Columns for Separation of Triazine Herbicides by Reversed Phase High Performance Liquid Chromatography
Monolithic and core-shell columns were comparatively evaluated for separation of deisopropylatrazine (DIA), deethylatrazine (DEA), hydroxyatrazine (HAT), simazine (SIM) and atrazine (ATR) under similar conditions of elution, flow rate and sample volume. Although both columns provided separation of the analytes with resolution > 1.5, the core-shell column exh
J. Braz. Chem. Soc.. Publicado em: 2015-11
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5. CONSTRUÇÃO DE UM DISPOSITIVO DE PRESSURIZAÇÃO A VÁCUO PARA A PREPARAÇÃO DE FASES ESTACIONÁRIAS MONOLÍTICAS VIA PROCESSO SOL-GEL
The filling of capillaries via the sol-gel process is growing. Therefore, this technical note focuses on disseminating knowledge acquired in the Group of Analytical Chemistry and Chemometrics over seven years working with monolithic stationary phase preparation in fused silica capillaries. We believe that the detailed information presented in this technical
Quím. Nova. Publicado em: 2015-01
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6. A numerical study on seismic response of self-centring precast segmental columns at different post-tensioning forces
Precast bridge columns have shown increasing demand over the past few years due to the advantages of such columns when compared against conventional bridge columns, particularly due to the fact that precast bridge columns can be constructed off site and erected in a short period of time. The present study analytically investigates the behaviour of self-centr
Lat. Am. j. solids struct.. Publicado em: 2014-10
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7. Physical and electrophoretic characterization of octadecyl methacrylate-based monolithic columns for use in capillary electrochromatography
Colunas de alta eficiência cromatográfica de origem monolítica orgânica foram obtidas para uso em eletrocromatografia capilar (CEC) utilizando uma mistura de monômeros (concentrações constantes) com diferentes proporções de solventes porogênicos (1,4- butanodiol com álcool isoamílico, álcool amílico ou cicloexanol, na presença ou ausência de
J. Braz. Chem. Soc.. Publicado em: 2013-03
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8. Metodologia analítica para determinação de triclosan e clorofenois por cromatografia a líquido de alta eficiência (HPLC) e cromatografia por injeção seqüencial (SIC) com uso de coluna monolítica e empacotada / Methodologies for the determination of triclosan and chlorophenols by high performance liquid chromatography (HPLC) and sequential injection chromatography (SIC) using packed and monolithic columns
Foram desenvolvidas metodologias de cromatografia a líquido de fase reversa baseadas em injeção sequencial (SIC) e em cromatografia a líquido de alta eficiência (HPLC) para determinação de triclosan em amostras de produtos de higiene pessoal e em estudos de adsorção em argilominerais naturais e modificados, visando determinar parâmetros de adsorç�
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 06/12/2011
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9. Desenvolvimento de um adsorvente contínuo supermacroporoso de troca catiônica para recuperação de lactoferrina de soro de leite / Development of a cation exchange solid supermacroporous adsorbent for lactoferrin recovery from whey
Whey proteins have functional, nutritional and technological properties promoting their use as ingredients and supplements. Sweet whey obtained from Minas Frescal cheese production and concentrated by ultrafiltration was used in the lactoferrin capture in a supermacroporous adsorbent. Supermacroporous monolithic columns have been prepared by radical cryo-cop
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 28/11/2011
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10. Fases estacionárias monolíticas para separações cromatográficas
Monolithic stationary phases represent a new generation of chromatographic separation media. These phases consist of a continuous separation bed prepared by in situ polymerization or consolidation inside the column tubing. In recent years, their simple preparation procedure, unique properties and excellent performance have attracted quite remarkable attentio
Química Nova. Publicado em: 2006-04
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11. Temperature-Modulated Array High-Performance Liquid Chromatography
Using novel monolithic poly(styrene-divinylbenzene) capillary columns with an internal diameter of 0.2 mm, we demonstrate for the first time the feasibility of constructing high-performance liquid chromatography arrays for the detection of mutations by heteroduplex analysis under partially denaturing conditions. In one embodiment, such an array can be used t
Cold Spring Harbor Laboratory Press.