Optical Synthesis
Mostrando 1-12 de 190 artigos, teses e dissertações.
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1. Synthesis of Conjugated Molecules Based on Dithienopyrrole Derivatives and Pyrene as Chemosensor for Mesotrione Detection
The conjugated molecules based on pyrene and dithienopyrrole derivatives including 4-(2-ethylhexyl)-2-(pyren-1-yl)-4H-dithieno[3,2-b:2’,3’-d]pyrrole (EP4HP) and 4-(2-ethylhexyl)-2,6-di(pyren-1-yl)-4H-dithieno[3,2-b:2’,3’-d]pyrrole (EDP4HP) have been successfully synthesized via C-H direct arylation reaction. The structures of these conjugated molecul
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Synthesis and characterization of α-SnWO4 powders obtained by microwave-assisted hydrothermal method
Abstract The structural, morphological, and optical properties of α-SnWO4 synthesized by microwave-assisted hydrothermal method at 150 °C for different times were investigated. XRD revealed the formation of the orthorhombic phase, without the presence of a secondary phase. The sample processed for 64 min showed a reduction in unit cell volume, suggesting a
Cerâmica. Publicado em: 2022
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3. Improving Photoluminescence Quantum Yield of CdTe Quantum Dots Using a Binary Solvent (Water + Glycerin) in the One-Pot Approach Synthesis
The present work describes the comparison of the optical and structural properties between CdTe quantum dots (QD) synthesized in water and in the binary solvent (water + glycerin) via one-pot approach synthesis. The optical properties of the nanocrystals obtained with different synthesis parameters were characterized by UV-visible and photoluminescence spect
J. Braz. Chem. Soc.. Publicado em: 2021-04
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4. Study of structural, optical, and morphological characteristics of manganese titanate (MnTiO3) obtained by combustion reaction using microwave energy
Abstract MnTiO3 is a semiconductor that has relevant dielectric and optical properties. For the synthesis of manganese titanate (MnTiO3) powders, the combustion method via microwave and subsequent calcination at 500, 700, and 900 °C were used. The structural, morphological, and optical properties of the samples were investigated. X-ray diffraction analyzes
Cerâmica. Publicado em: 2021-03
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5. Synthesis, Characterization and Exchange Reactions of Layered Double Hydroxides of Copper and Aluminum, Intercalated with Sulfate
Layered double hydroxides (LDHs) of Cu:Al in the molar ratio of 2:1, intercalated with sulfate, sulfate/(Li+, Na+, K+ or NH4+), NO3- and CO32-, were synthesized by co-precipitation with increasing pH. The materials were submitted to exchange reactions using B2SO4 (B = Li+, Na+, K+, NH4+) solutions in an attempt to replace previously intercalated cations or i
J. Braz. Chem. Soc.. Publicado em: 2021-01
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6. A Straightforward Synthesis of Enantiopure (1S,2R)-Ephenamine
An enantioselective six-step synthesis of (1S,2R)-ephenamine starting from readily available chiral amino acid is disclosed presenting 26% overall yield and high optical purity. The use of chiral phenylglycine as starting material was also studied and did not present satisfactory results due to a very sensitive a-carbonyl/benzylic stereogenic center that, in
J. Braz. Chem. Soc.. Publicado em: 2020-12
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7. MÉTODO MANUAL PARA DEPOSIÇÃO DE TINTAS FOTOLUMINESCENTES BASEADAS EM LOFS MISTAS APLICADO A CODIFICAÇÃO DE DOCUMENTOS
In this work, the process of synthesis of Metal-Organic Frameworks containing lanthanide ions (LOFs), accelerated via a precipitating agent, capable of accelerating the process of nucleation of MOF crystals, in order to explore the optical properties of this precursor solution (SP_Gd/EU-MOF), as a quick-response photoluminescent material in the coding of off
Quím. Nova. Publicado em: 2020-12
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8. SÍNTESE E CARACTERIZAÇÃO DE PONTOS QUÂNTICOS AMBIENTALMENTE AMIGÁVEIS, UM MEIO SIMPLES DE EXEMPLIFICAR E EXPLORAR ASPECTOS DA NANOCIÊNCIA E NANOTECNOLOGIA EM CURSOS DE GRADUAÇÃO
Nanotechnologies and nanomaterials are very current and interesting topics and can be used as interdisciplinary tools in education. They can be used to work in a practical and interesting way with lots of subjects. In chemistry teaching it can be particularly important to consolidate the nanomaterials, nanotechnology and characterization teaching. Among the
Quím. Nova. Publicado em: 2020-06
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9. Synthesis of New Phenolic-Schiff Base and Its Application as Antioxidant in Soybean Biodiesel and Corrosion Inhibitor in AISI 1020 Carbon Steel
New Schiff base compound N, N’-bis-(4-hexadecanate)-salicylethylenediamine (named IM) was synthesized, and characterized via infrared and nuclear magnetic ressonance spectroscopies. IM was tested as corrosion inhibitor and antioxidant in soybean biodiesel. Corrosion studies were developed with AISI 1020 carbon steel in a three-step accelerated corrosion as
J. Braz. Chem. Soc.. Publicado em: 2020-03
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10. Evaluation of the Influence of the Substituting Cation on the Structural and Morphological Properties of the New Garnet Sm3−xREExFe5O12 (REE = Dy, Gd and Lu)
Rare earth garnets (REE3Fe5O12) have magnetic-electric and optical properties that can be used in transmitters, microwave and data storage devices. These properties depend mainly on partial or total substitution of the cationic sites, as well as by the synthesis method used. Therefore, in this work was studied the influence of the substituting cation on the
Mat. Res.. Publicado em: 20/01/2020
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11. ONE-POT DIASTEREOSELECTIVE SYNTHESIS OF CHIRAL TRICYCLIC L-CYSTEINE AND D-PENICILLAMINE DERIVATIVES: A LABORATORY EXPERIMENT
A one-pot diastereoselective synthesis of thiazolidine-ring fused systems derived from enantiomerically pure amino acids, L-cysteine or D-penicillamine, and achiral succindialdehyde is described as an experiment to be carried out by upper-division undergraduate students in a laboratory classroom. Reactions were performed under mild conditions, the products w
Quím. Nova. Publicado em: 2020-01
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12. Solvothermal Synthesis of Cerium-Doped Titania Nanostructured Materials Modified with Acetylacetone for Solar-Driven Photocatalysis
This study reports the preparation of nanostructured cerium-doped titanium dioxide photocatalysts containing different cerium concentrations by a modified sol-gel route involving the use of acetylacetone. The nanocrystalline powders had their structural, morphological, and optical properties characterized by X-ray diffraction, vibrational and Raman spectrosc
J. Braz. Chem. Soc.. Publicado em: 2020-01