Powders Synthesis
Mostrando 1-12 de 105 artigos, teses e dissertações.
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1. Synthesis of delafossite CuCrO2 via solution combustion method and its acid functionalization for biodiesel production
Abstract CuCrO2 was synthesized by solution combustion synthesis (SCS) and applied as a heterogeneous catalyst to produce soybean biodiesel. The combustion reaction was carried out using urea as a fuel, and copper (II) and chromium (III) nitrates as precursors. After the powders’ obtention, these were calcined and functionalized in an acidic medium. The po
Cerâmica. Publicado em: 2023
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2. Synthesis and characterization of α-SnWO4 powders obtained by microwave-assisted hydrothermal method
Abstract The structural, morphological, and optical properties of α-SnWO4 synthesized by microwave-assisted hydrothermal method at 150 °C for different times were investigated. XRD revealed the formation of the orthorhombic phase, without the presence of a secondary phase. The sample processed for 64 min showed a reduction in unit cell volume, suggesting a
Cerâmica. Publicado em: 2022
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3. Synthesis and characterization of niobium-doped fish scale-derived hydroxyapatite by physical ultrasound interference
Abstract Fish scales of the Arapaima gigas (pirarucu) species were heat-treated to obtain natural hydroxyapatite (HAp), and it was doped with niobium (Nb) by physical ultrasound interference to confirm an effective route to the production of Nb-doped HAp powders. The effect of ultrasound application on doping was investigated. The structure of the powders wa
Cerâmica. Publicado em: 2021-03
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4. Study of structural, optical, and morphological characteristics of manganese titanate (MnTiO3) obtained by combustion reaction using microwave energy
Abstract MnTiO3 is a semiconductor that has relevant dielectric and optical properties. For the synthesis of manganese titanate (MnTiO3) powders, the combustion method via microwave and subsequent calcination at 500, 700, and 900 °C were used. The structural, morphological, and optical properties of the samples were investigated. X-ray diffraction analyzes
Cerâmica. Publicado em: 2021-03
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5. Synthesis of a Ce-Based MOF-76 with High Yield: A Study of Reaction Parameters Based on a Factorial Design
The purpose of this work was to optimize the synthesis yield of {[Ce(BTC)(H2O)]·DMF}n, a metal-organic framework (MOF)-76 family member, by solvothermal method. CeCl3.7H2O and 1,3,5-benzenetricarboxylic acid, 2:1 molar proportion, were added to N, N-dimethylformamide (DMF). Reaction time and temperature were evaluated to optimize the synthesis through a fac
J. Braz. Chem. Soc.. Publicado em: 2020-03
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6. Solvothermal Synthesis of Cerium-Doped Titania Nanostructured Materials Modified with Acetylacetone for Solar-Driven Photocatalysis
This study reports the preparation of nanostructured cerium-doped titanium dioxide photocatalysts containing different cerium concentrations by a modified sol-gel route involving the use of acetylacetone. The nanocrystalline powders had their structural, morphological, and optical properties characterized by X-ray diffraction, vibrational and Raman spectrosc
J. Braz. Chem. Soc.. Publicado em: 2020-01
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7. Obtenção de ferritas de cálcio dopadas com cromo visando aplicação em esmaltes transparentes brilhante e mate
RESUMO Este trabalho tem como objetivo obter óxidos com estrutura tipo espinélio de composição CaFe1,8Cr0,2O4 pelo método gelatina, visando aplicação em esmaltes transparentes brilhantes e mate. Os pós precursores, resultantes do processo de síntese, foram calcinados a 600 °C e a 800 °C para a obtenção da fase espinélio. Os pós foram caracteri
Matéria (Rio J.). Publicado em: 25/11/2019
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8. Síntese de perovskitas tipo LaAl1-xCrxO3 para aplicação em esmalte transparente
RESUMO No Brasil, estudos sobre pigmentos cerâmicos ainda são bastante escassos. Por esta razão, grande parte dos pigmentos consumidos pela indústria cerâmica são importados dos países europeus. Outra parte destes pigmentos são obtidos pela rota cerâmica, entretanto, esta rota de síntese resulta em pigmentos com propriedades bastante heterogêneas,
Matéria (Rio J.). Publicado em: 25/11/2019
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9. Molten Salt Synthesis of Bi2WO6 Powders and its Visible-Light Photocatalytic Activity
Bi2WO6 powders were synthesized by the molten salt method at 250-350 ºC using the mixture of Bi(NO3)3·5H2O and Na2WO4·2H2O as a precursor, and the mixture of LiNO3 and NaNO3 with a molar ratio of 27:33 as a molten salt, respectively. The effects of temperature and salt amount on the phase composition, morphology and photocatalytic activity under the visib
Mat. Res.. Publicado em: 21/10/2019
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10. Nanoparticles of Ni1-x Znx Fe2 O4 used as Microwave Absorbers in the X-band
Ferrites nanoparticles of Ni1-xZnxFe2O4 ferrites with x varying between 0 and 1, in steps of 0.2, were obtained by solution combustion synthesis (SCS) and dispersed in oil paint at the concentrations of 10, 20, 30 and 40% by ferrite weight of ferrite, with the aim of producing electromagnetic wave absorbing composites, in the X band (8-12 GHz). The ferrite p
Mat. Res.. Publicado em: 21/10/2019
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11. Estudio de las propiedades, estructurales, morfológicas y ópticas de nanopartículas de Cr2O3 sintetizadas por procesos de combustión de un solo paso y diferentes combustibles
ABSTRACT This research presents a novel one–step solution combustion synthesis to obtain nano-structured Cr2O3 from chrome nitrate solution and one fuel such as aspartic acid (Asp) or Lysine (Lys), or Autor Restrihydroxymethylaminomethane (Tris) or ethylenediaminetetraacetic acid (Edta). Once obtained, the ashes were calcined at 500°C. The powders were ch
Matéria (Rio J.). Publicado em: 16/09/2019
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12. Influência do tipo de solvente na síntese de mulita pelo método Pechini
Resumo Mulita é um aluminossilicato com grande importância na tecnologia cerâmica. Sua síntese através de métodos químicos tem sido extensivamente estudada, no entanto, não se observam estudos da sua obtenção pelo método Pechini. Assim, este estudo teve por objetivo a síntese de mulita por meio deste método. Foi avaliada a influência de diverso
Cerâmica. Publicado em: 15/08/2019