Response Surface Analysis
Mostrando 1-12 de 711 artigos, teses e dissertações.
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1. Analysis of Al2O3-ZrO2 ceramic insert in turning process of Ti-6Al-4V alloy using grey Taguchi-based response surface methodology (GT-RSM)
Abstract The present investigation aimed at a sustainable green turning operation of Ti-6Al-4V alloy using multi-objective optimization of surface roughness, tool flank wear, material removal rate, and tool wear loss with cutting speed, feed rate, and depth of cut as input parameters. The experiments were performed on a CNC lathe machine using an alumina-zir
Cerâmica. Publicado em: 2022
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2. In vivo Administration of Testosterone Propionate in Cattle Analyzed by High Performance Liquid Chromatography-Tandem Mass Spectrometry: An Enzymatic Hydrolysis Study and Drug Abuse Issues
This study involved an animal experiment in which testosterone propionate was intramuscularly injected into four steers, and the ensuing urine samples were analyzed using high-performance liquid chromatography-tandem mass spectrometry. The enzymatic hydrolysis conditions were analyzed using analysis of variance (ANOVA) and response surface methodology employ
Journal of the Brazilian Chemical Society. Publicado em: 2022
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3. Additive Manufacturing towards the Fabrication of Greener Electrochemical Sensors for Antioxidants
Additive manufacturing is an emerging tool that has contributed to the sustainable fabrication of devices in several areas based on the concept of “zero waste”. Considering extrusion-based manufacturing (or 3D printing), polylactic acid (PLA) has been highlighted due to its biodegradability, obtention from renewable sources, and compatibility for 3D prin
Journal of the Brazilian Chemical Society. Publicado em: 2022
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4. A novel fluorescence sensor for the detection of chloride ion in artificial sweat and environmental water with nitrogen-doped graphene quantum dots
A new fluorescent detection route for chloride ion was designed with Nitrogen-doped graphene quantum dots (N-GQDs), which were prepared by a traditional hydrothermal method with citric acid as carbon source and urea as nitrogen source. The prepared N-GQDs solution was light yellow, and the freeze-dried solid was black. It emitted blue light under ultraviolet
Química Nova. Publicado em: 2022
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5. Optimization of potato starch gel formulation as green alternative of animal-sourced gelatin
Abstract This study was aimed at optimization of potato starch gel preparation process by response surface methodology and various process parameters were optimized for textural, gelation and sensory properties. 3D response surface and contour plots showed that independent variables, such as extraction time, extraction temperature and potato starch concentra
Food Sci. Technol. Publicado em: 2021-09
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6. Multivariate Optimization Applied to the Synthesis of Meglumine Antimoniate with Low Levels of Trivalent Antimony
Meglumine antimoniate (MA) is a pentavalent antimony (SbV) drug recommended for the treatment of leishmaniasis. It is known that the trivalent antimony (SbIII) present as a residue in MA contributes to the drug side effects. In this article, multivariate optimization was used in the synthesis of MA in order to obtain a drug with low levels of SbIII. Four var
J. Braz. Chem. Soc.. Publicado em: 2021-08
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7. A Comparison of the Photolytic and Photocatalytic Degradation of Triclosan: Identification of Transformation Products and Ecotoxicity Evaluation
Triclosan (5-chloro-2-(2,4-dichlorophenoxy)phenol) is commonly used as an antibacterial agent in various industrial products and is often detected in wastewater effluent. Comparison was made for triclosan degradation by photolysis and TiO2 photocatalysis (under UV irradiation (125 W)) based on analysis of transformation products, together with ecotoxicity ev
J. Braz. Chem. Soc.. Publicado em: 2021-08
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8. Optimization and Study of the Response Surface of Properties for the Synthesis of ZSM-5 Zeolites with Hierarchical Pore Structure Obtained by Desilication
Hierarchical ZSM-5 zeolites were prepared by alkali treatment (desilication) at two temperatures, two reaction times, and two NaOH concentrations. A 23 factorial design was used to study the effect of these variables on the crystallinity, microporosity, and mesoporosity of the zeolite due to the desilication treatment. The factorial design analysis showed th
J. Braz. Chem. Soc.. Publicado em: 2021-06
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9. OPTIMIZATION OF BREWING WASTE’S (TRUB) PHENOLIC COMPOUNDS EXTRACTION BY ULTRASOUND ASSISTED USING RESPONSE SURFACE METHODOLOGY
The brewing waste, also known as trub, is an abundant by-product of the brewing industry. Such material presents high levels of phenolic compounds, which promote antioxidant, antimicrobial and antifungal effects, turning the trub economically attractive. In this study, the trub’s phenolic compounds were extracted by ultrasound-assisted extraction technolog
Quím. Nova. Publicado em: 2021-04
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10. Response surface optimization of polysaccharide extraction from Galla Chinensis and determination of its antioxidant activity in vitro
Abstract Galla Chinensis was a traditional Chinese medicine used as an ingredient in many prescriptions for the treatment of oxidant damage-associated symptoms in China. The current research on the isolation of polysaccharides from Galla Chinensis and their antioxidant activities still remain as an ongoing challenge. The purpose of this study is to develop a
Food Sci. Technol. Publicado em: 2021-03
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11. Green Extraction Optimization of Bioactive Compounds from Rosemary (Rosmarinus officinalis L.) Using Response Surface Methodology
Rosemary (Rosmarinus officinalis L.) is known for its bioactive compounds with high antioxidant potential and pharmacological properties, such as antibacterial, antidepressant and anti-inflammatory. These properties are attributed to the presence of (poly)phenolic compounds. In the literature there is no extraction of these compounds with a totally non-toxic
J. Braz. Chem. Soc.. Publicado em: 2020-12
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12. Preparation of antioxidant peptides from hairtail surimi using hydrolysis and evaluation of its antioxidant stability
Abstract In this study, antioxidant peptides were prepared from hairtail surimi by hydrolysis. Response surface methodology coupled with a Box-Behnken design was applied to optimize hydrolysis conditions. The optimum conditions were determined as: 12.1 h incubation time, 44.74 °C incubation temperature and enzyme concentration 1858.85 U/g. The amino acid co
Food Sci. Technol. Publicado em: 2020-12