Reversed Stationary Phases
Mostrando 1-12 de 23 artigos, teses e dissertações.
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1. Per-Aqueous Liquid Chromatography for the Separation of Polar Compounds Preparation and Characterization of Poly(ethylene oxide co dimethylsiloxane) Based Stationary Phase
Poly(ethylene oxide-co-dimethylsiloxane) was thermally immobilized on silica particles-Si(PEO)-to separate small polar compounds with water-rich mobile phases. Poly(ethylene oxide-co-dimethylsiloxane) content on Si(PEO) stationary phase was optimized using a central composite design. Infrared spectroscopy, scanning electron microscopy, and thermogravimetric
Journal of the Brazilian Chemical Society. Publicado em: 2022
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2. Self-Immobilization of Poly(methyltetradecylsiloxane) onto Metalized Silica Particles as Stationary Phases for HPLC
This work presents a study of the sorption of a pre-synthesized polysiloxane, poly(methyltetradecylsiloxane) - PMTDS, onto zirconized and titanized-silica particles that results in efficient stationary phases for reversed phase liquid chromatography. The sorbed materials, after 6 days at room temperature without any chemical or physical agent, denominated as
J. Braz. Chem. Soc.. Publicado em: 2016-06
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3. O desafio de analisar solutos básicos por cromatografia líquida em modo reverso: algumas alternativas para melhorar as separações
This review considers some of the difficulties encountered with the analysis of basic solutes using reversed-phase chromatography, such as detrimental interaction with stationary phase silanol groups. Methods of overcoming these problems in reversed-phase separations, by judicious selection of the stationary phase and mobile phase conditions, are discussed.
Química Nova. Publicado em: 2012
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4. Preparação e caracterização de fase estacionária reversa fenil-propil-metil-siloxano, imobilizada por micro-ondas, para cromatografia líquida de alta eficiência / Preparation and characterization of microwave-immobilized phenyl-propyl-methyl-siloxane stationary phase for reversed-phase high-performance liquid chromatography
Novas fases estacionárias (FE) para Cromatografia Líquida de Alta Eficiência em fase reversa (CLAE-FR) foram preparadas a partir da sorção e imobilização por micro-ondas do copolímero poli(2- fenilpropil)metilsiloxano (PFPMS) sobre suporte de sílica Kromasil (tipo B, esférica, 5 mm). A FE preparada com carga do copolímero de 50%, imobilizada a 540
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 01/08/2011
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5. Fases estacionárias para cromatografia líquida de alta eficiência em fase reversa por imobilização térmica do poli(2-fenilpropil) metilsiloxano sobre sílica / Stationary phases for reversed-phase high-performance liquid chromatography using thermal immobilization of poly (phenylpropyl) methylsiloxane onto silica
Este trabalho apresenta o desenvolvimento de fases estacionárias (FE) para utilização em Cromatografia Líquida de Alta Eficiência em Fase Reversa (CLAE-FR) a partir da imobilização térmica de poli (2-fenilpropil) metilsiloxano (PFPMS) sobre suporte de sílica. Diferentes quantidades de copolímero foram avaliadas, alcançando-se um bom desempenho cro
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 01/03/2011
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6. Preparo, caracterização e aplicação de fases estacionárias de poli(dimetilsiloxano-co-metilfenilsiloxano) sorvidas e imobilizadas sobre sílica e sílica zirconizada / Preparation, characterization and application of stationary phases based on poly(dimethylsiloxane-co-methylphenylsiloxane), sorbed and immobilized onto silica and zirconized silica
This work describes the development of new stationary phases (SP) based on poly(dimethylsiloxane-co-methylphenylsiloxane) sorbed and immobilized onto silica and zirconized silica for reversed phase high performance liquid chromatography. The polymer was immobilized by thermal treatment at 140 °C during 6 h, which were the conditions that produced SP with th
IBICT - Instituto Brasileiro de Informação em Ciência e Tecnologia. Publicado em: 25/02/2011
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7. Fases estacionárias modernas para cromatografia líquida de alta eficiência em fase reversa
This review first discusses the limitations of many of the supports and stationary phases used in reversed phase high performance liquid chromatography and then describes those, developed more recently, that present better stabilities and more versatile selectivities. Emphases will be given to stationary phases that use higher purity silicas, hybrid silicas,
Química Nova. Publicado em: 2010
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8. Determinação da espessura da camada polimérica de fases estacionárias imobilizadas para cromatografia líquida de alta eficiência por termogravimetria
This paper presents a simple and practical thermogravimetric method for determining the layer thickness of immobilized polymer stationary phases used in reversed-phase high-performance liquid chromatography. In this method, the weight loss of different polysiloxanes immobilized onto chromatographic supports, determined over the temperature range 150-650 ºC,
Química Nova. Publicado em: 2008
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9. Desenvolvimento de fases estacionarias para cromatografia liquida de alta eficiencia em fase reversa a partir da adsorção e imobilização do poli(metiltetradecilsiloxano) sobre silica metalizada / Development of stationary phases for reservesed-phase hight-performance liquid chromatography by adsortion and immobilization of poly(metyltetradecysiloxane) onto metalized silica supports
This work presents the development of stationary phases for used in Reversed-Phase High-Performance Liquid Chromatography (RP-HPLC) by sorption and immobilization of poly(methyltetradecylsiloxane) (PMTDS) onto metalized (zirconized and titanized) silica supports. The preparation of metalized silica supports was optimized using experimental design. Two immobi
Publicado em: 2006
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10. Desenvolvimento de fases estacionarias de polaridade intermediaria para cromatografia liquida de alta eficiencia em fase reversa / Development of intermediate polarity stationary phases for reversed phase high performance liquid chromatography
Este trabalho visa o desenvolvimento de fases estacionárias reversas para utilização em Cromatografia Líquida de Alta Eficiência (CLAE), a partir de sílica Kromasil zirconizada (suporte) e dos polímeros polietilenoglicol 1000, poli(metil)decil (2-5%) difenilsiloxano e polidimetilsiloxano aminopropil (fase líquida). O suporte zirconizado foi sintetiza
Publicado em: 2005
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11. Novas fases estacionárias à base de sílica para cromatografia líquida de alta eficiência
The present work reviews recent advances in the preparation of new reversed phase packing materials such as sterically protected, bidentate, hybrid organic-inorganic and monolithic phases and phases containing embedded polar groups. The bonding chemistry involved in the preparation of these phases as well as their advantages over conventional C8 and C18 reve
Química Nova. Publicado em: 2004-04
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12. Preparação de colunas para cromatografia liquida de alta eficiencia recheadas com polissiloxanos (C1, C8 e C14) imobilizados sobre particulas de silica porosa de 5mum
In this work, reversed phases for High-Performance Liquid Chromatography (HPLC) were obtained by deposition of polysiloxanes with different lateral chains, C1 (polydimethylsiloxane), C8 (polymethyloctylsiloxane) and C14 (polymethyltetradecylsiloxane), in HPLC silica particles, followed by immobilizatíon using different processes: thermal treatment, self-imm
Publicado em: 2004