Solid Oxide
Mostrando 1-12 de 179 artigos, teses e dissertações.
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1. Reduced Graphene Oxide-Cadmium Sulfide Quantum Dots Nanocomposite Based Dispersive Solid Phase Microextraction for Ultra-Trace Determination of Carbamazepine and Phenobarbital
This research presents a fast, sensitive, and selective ultrasound-assisted dispersive solid phase microextraction technique for simultaneous preconcentration and determination of ultra-trace amount of carbamazepine and phenobarbital. Reduced graphene oxide sheets decorated with cadmium sulfide quantum dots was synthesized, characterized, and used as a high
J. Braz. Chem. Soc.. Publicado em: 2021-04
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2. Bioactive Bioflavonoids from Platonia insignis (Bacuri) Residues as Added Value Compounds
Platonia insignis fruit, popularly known as bacuri, is traditionally used in folk medicine for its anti-inflammatory and antioxidant properties. Therefore, this study determined the chemical composition and biological activities of the bacuri’s shell and seeds extracts, considered residues from its consumption and industrial uses. Four biflavonoids (GB-2a,
J. Braz. Chem. Soc.. Publicado em: 2021-04
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3. Magnetic Solid-Phase Microextraction for Lead Detection in Aqueous Samples Using Magnetite Nanoparticles
A magnetic solid-phase microextraction procedure was developed to detect lead in aqueous samples by flame atomic absorption spectrometry (FAAS). Fe3O4 nanoparticles were synthesized by coprecipitation and the crystalline phase was confirmed by X-ray diffraction. The point of zero charge (PZC) indicated that the oxide surface was negatively charged at pH leve
J. Braz. Chem. Soc.. Publicado em: 2020-01
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4. Immunomodulation Properties of Solid-State Fermented Laetiporussulphureus Ethanol Extracts in Chicken Peripheral Blood Monocytes In Vitro
ABSTRACT Laetiporus sp. is recognized as a fungal species traditionally used for medicinal purposes. This study investigated the in-vitro effects of solid-state fermented Laetiporussulphureus ethanol extracts (LSE) for their immunomodulatory potential. Bioactive levels detected in the LSE on different days throughout the fermentation period revealed that the
Braz. J. Poult. Sci.. Publicado em: 20/12/2019
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5. Phase and microstructural analysis of NdTi0.8M0.2O3.4 (M = Al, Ga) microwave ceramics
ABSTRACT In this paper, we report the characterization of NdTi0.8M0.2O3.4 (M = Ga, Al) ceramics prepared via mixed oxide solid state sintering route. X-ray diffraction analysis of the samples revealed the formation of single phase for NdTi0.8Ga0.2O3.4 sample while secondary phase was formed in the case of NdTi0.8Al0.2O3.4. Microstructural analysis of the sam
Matéria (Rio J.). Publicado em: 25/11/2019
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6. Interrelation Among Morphology, Mechanical Properties and Oxidation Behavior of NbxAlyNz Thin Films
NbxAlyNz thin films were deposited by magnetron sputtering reactive technique with (y/x+y) ratio varying from 0 to 0.4, in order to maintain aluminum atoms inside NbN matrix in solid solution. GAXRD analyses revealed that the crystalline phase obtained for NbxAlyNz thin films was B1-NbN with a lattice constant shrinkage as Al concentration at these coatings
Mat. Res.. Publicado em: 07/11/2019
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7. Transmissive to Dark Electrochromic and Fluorescent Device Based on Poly(fluorene-bisthiophene) Derivative
Films of a poly(fluorene-bisthiophene) derivative, named PFBT, were electrodeposited onto indium tin oxide (ITO) electrodes and their electrochromic and fluorescence properties were investigated. Such films displayed color variation from yellow, in the neutral state, to green, in the oxidized state, as shown by tracking of the CIE (Commission Internationale
J. Braz. Chem. Soc.. Publicado em: 24/10/2019
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8. Influence of Yttria-Stabilized Zirconia on Microstructure and Electrical Properties of Doped Lanthanum Gallate
Lanthanum gallate with partial substitutions for strontium and magnesium shows higher ionic conductivity than traditional ionic conductors such as yttria-stabilized zirconia (8YSZ), and has been considered for application as solid electrolyte and electrode in Solid Oxide Fuel Cells operating at intermediate temperatures (500-700ºC). Parallel to the developm
Mat. Res.. Publicado em: 01/08/2019
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9. Solid Phase Extraction Using SiO2/Al2O3/TiO2 Ternary Oxide for Cu2+ Preconcentration
The present work aims at studying the preconcentration of Cu2+ ions by solid phase extraction using SiO2/Al2O3/TiO2 ternary oxide as adsorbent material. This methodology consists of the affinity of the analyte for the adsorbent material and its subsequent elution with the least amount of solvent. Subsequently, the aqueous phase containing the extracted analy
J. Braz. Chem. Soc.. Publicado em: 04/07/2019
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10. Application of SnO2 Nanoparticles and Zeolites in Coal Mine Methane Sensors
We evaluated solid-state sensors (MOS) manufactured using nanostructured tin oxide (SnO2) obtained by different synthesis methods for selectivity, response and repeatability at different operating temperatures and methane concentrations. In addition, Zeolite 13X pellets were placed in front of the sensors to improve CH4 selectivity in the presence of CO2. Th
Mat. Res.. Publicado em: 27/05/2019
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11. Nb-doped Ti2O3 Films Deposited Through Grid-Assisted Magnetron Sputtering on Glass Substrate: Electrical and Optical Analysis
Abstract Niobium doped dititanium trioxide (Ti2O3:Nb) films were deposited on glass substrates, through grid-assisted magnetron sputtering. The Ti2O3:Nb films were characterized by X-ray diffraction (XRD), electrical conductivity and optical properties. Film deposition was carried out in two different substrate bias modes: DC and unipolar pulsed. Results sho
Mat. Res.. Publicado em: 24/01/2019
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12. Effect of blisters and rims on radial hydride precipitation in fuel elements under dry storage conditions
ABSTRACT Hydrogen enters in Zry clads during fuel element life in service; when hydrogen exceeds the terminal solid solubility, circumferential hydrides are precipitated. In the presence of thermal gradients, produced for instance by oxide spallation, localized concentration of hydrides - known as blisters - can be formed. Due to the fact that zirconium hydr
Matéria (Rio J.). Publicado em: 19/07/2018